Assessor Resource

MSL975010
Perform fire assay techniques

Assessment tool

Version 1.0
Issue Date: May 2024


This unit of competency covers the ability to safely extract a range of precious metals from their host matrices in readiness for analysis. The unit also covers the ability to select and/or modify laboratory methods to suit particular ores and to ensure total recovery.

This unit of competency is applicable to laboratory personnel working in the mineral assay industry sector.

While no specific licensing or certification requirements apply to this unit at the time of publication, laboratory operations are governed by relevant legislation, regulations and/or external accreditation requirements. Local requirements should be checked.

You may want to include more information here about the target group and the purpose of the assessments (eg formative, summative, recognition)



Evidence Required

List the assessment methods to be used and the context and resources required for assessment. Copy and paste the relevant sections from the evidence guide below and then re-write these in plain English.

Elements describe the essential outcomes.

Performance criteria describe the performance needed to demonstrate achievement of the element.

1

Classify ore samples and select fluxing method

1.1

Review client request to identify sample/analysis requirements, preparation methods and equipment involved

1.2

Inspect samples, compare with specifications, record and report any discrepancies

1.3

Conduct visual and simple chemical tests to identify the type of sample and sulphide concentrations

1.4

Review client sample/analysis history and identify possible chemical interferences

1.5

Decide whether non-standard fluxing is required

1.6

Select sample weight and flux to optimise precious metal recovery and purity

2

Prepare for precious metal recovery

2.1

Identify hazards and workplace safety procedures associated with the sample, preparation methods, reagents and equipment

2.2

Examine the recommended preparation method to identify the critical steps that will affect the quality of analytical results

2.3

Plan parallel work sequences to optimise the throughput of multiple sets of samples

2.4

Assemble all required equipments, materials, reagents and check they are fit for purpose

3

Recover precious metals from ore sample

3.1

Weigh required amounts of sample and flux components to achieve an acceptable button and fluid slag

3.2

Select the type and size of pot to suit sample method and client requirements

3.3

Mix charge to ensure homogeneity and optimal collection of precious metal

3.4

Set and monitor furnace temperature/time to ensure complete fusion

3.5

Separate slag and button with minimal loss of lead collector

3.6

Maintain sequencing in order to track samples, buttons and prills throughout the recovery process

3.7

Separate lead collector from the required precious metal and check for contamination, losses and evidence of other precious metals

3.8

Minimise personal exposure to hazards and the release of collectors to the work environment

3.9

Collate laboratory documentation and the prepared sample and present for analysis

4

Troubleshoot and correct failed recovery

4.1

Monitor all stages of recovery for indicators of potential loss

4.2

Recognise undesirable recovery conditions and decide whether the process requires correction

4.3

Choose an appropriate corrective action and re-start the process

4.4

Document any adjustments made to standard methods and re-sequencing of samples

4.5

Seek advice when problems are beyond scope of responsibility or knowledge

5

Perform daily maintenance of assay equipment

5.1

Segregate and dispose of waste in accordance with workplace requirements

5.2

Grade and inspect pots using established criteria prior to storage for re-use

5.3

Inspect furnaces for cracks, unserviceable components and remove slag

5.4

Inspect and clean extractive systems

5.5

Report defective equipment and consumable requirements to appropriate personnel

Evidence of competence in this unit must satisfy all of the requirements of the elements and performance criteria, and include demonstration of:

safely performing fire assay techniques to extract a range of precious metals from their host matrices in readiness for analysis on at least three (3) occasions

interpreting and closely following standard recovery methods

selecting and modifying laboratory methods to suit particular ores and to ensure total recovery

accurately weighing samples and flux components

maintaining close attention to technical and safety requirements in a physically demanding hazardous environment

maintaining sequential control of samples through all recovery stages

optimising work flow to ensure efficiency of recovery for multiple client samples

recognising and identifying the cause of non-acceptable received and fused samples, buttons and prills

identifying indicators of poor recovery and contamination

applying knowledge of mineral chemistry and fire assay techniques to solve recovery and contamination problems

keeping accurate and complete records, including:

pour sheets (date, time, client, pour number and preparation method)

number of pots, positions of sample, blank and check in rack

adjustments made to standard preparation methods for specific samples

analytical method

assay data

minimising rework, waste and environmental impacts

safely collecting and disposing of all waste responsibly

recognising hazards, using workplace safety procedures and safety equipment to work safely at all times.

Must provide evidence that demonstrates knowledge of:

chemical and physical principles relating to:

fusion of mineral ores

cupellation

parting and digestion processes

expected physical and chemical properties of materials at each recovery stage

standard methods for the fire assay of a range of precious metal ores relevant to job role

criteria for an 'acceptable' button, including:

one piece, mass >20g and <50g

malleable

separates cleanly from slag

free of undecomposed ore, matte and speiss

causes of contamination, including:

poorly made cupels

base metals (copper (Cu), nickel (Ni), zinc (Zn) and bismuth (Bi))

arsenic (As), sulphur (S), antimony (Sb), selenium (Se), tellurium (Te) and chromium (Cr)

scoria

sprouting

indicators of potential loss and the corrective actions, including:

viscous slag (check furnace temperature, adjust flux and lower charge weight)

lead shotting (adjust flux and lower charge weight to compensate for high oxides, silicates and chromites)

sulphides (adjust fusion time and adjust sample weight and/or flux)

matte, speiss (adjust sample weight and flux)

incomplete fusion (adjust sample weight and/or flux)

unacceptable button (adjust sample weight and/or flux)

inquartation (add 3 parts silver (Ag) to prill, wrap in lead foil and re-cupel)

workplace safety procedures and operation of safety equipment

function and operation of assay/equipment used as part of job role

workplace and/or legal traceability requirements

relevant hazards, work health and safety (WHS) and environment requirements.

Judgment of competence must be based on holistic assessment of the evidence. Assessment methods must confirm consistency of performance over time, rather than a single assessment event.

This unit of competency is to be assessed in the workplace or a simulated workplace environment. A simulated workplace environment must reflect realistic operational workplace conditions that cover all aspects of workplace performance, including the environment, task skills, task management skills, contingency management skills and job role environment skills.

Foundation skills are integral to competent performance of the unit and should not be assessed separately.

Assessment processes and techniques must be appropriate to the language, literacy and numeracy requirements of the work being performed and the needs of the candidate.

Knowledge evidence may be collected concurrently with performance evidence or through an independent process, such as workbooks, written assessments or interviews (provided a record is kept in each case).

This unit of competency may be assessed with:

MSL975020 Apply routine spectrometric techniques

Holistic assessment methods include:

observation of the candidate

review of quality control performance and analytical results traceable to assay samples prepared by the candidate

review of sample records prepared by the candidate

feedback from supervisors, peers and/or clients about the candidate’s ability to safely and efficiently extract a range of precious metals from their host matrices in readiness for analysis, provide acceptable buttons and prills, and troubleshoot and correct common recovery failures

written/oral questioning about relevant mineral chemistry principles, precious metal recovery steps, typical problems and corrective actions.

Access is required to instruments, equipment, materials, workplace documentation, procedures and specifications associated with this unit, including, but not limited to:

client requests/documentation, including client profile, sample identification, sample receipt, storage and analyses, and required preparation method/and service charges

a variety of precious metal ore samples

fire assay methods, examples of assay records, equipment, materials and reagents

assay equipment, including:

mixing equipment and balances

fusion and muffle furnaces and associated spares

temperature sensors and hotplates

compressed air service, extraction systems and fuel supply lines

pots, cupels, pouring equipment, pot loader, trolleys, moulds, tongs and hammers

safety equipment and workplace safety procedures.

Assessors must satisfy the assessor competency requirements that are in place at the time of the assessment as set by the VET regulator.

The assessor must demonstrate both technical competence and currency.

Technical competence can be demonstrated through:

relevant VET or other qualification/Statement of Attainment AND/OR

relevant workplace experience.

Currency can be demonstrated through:

performing the competency being assessed as part of current employment OR

having consulted with a laboratory about performing the competency being assessed within the last twelve months.


Submission Requirements

List each assessment task's title, type (eg project, observation/demonstration, essay, assingnment, checklist) and due date here

Assessment task 1: [title]      Due date:

(add new lines for each of the assessment tasks)


Assessment Tasks

Copy and paste from the following data to produce each assessment task. Write these in plain English and spell out how, when and where the task is to be carried out, under what conditions, and what resources are needed. Include guidelines about how well the candidate has to perform a task for it to be judged satisfactory.

Elements describe the essential outcomes.

Performance criteria describe the performance needed to demonstrate achievement of the element.

1

Classify ore samples and select fluxing method

1.1

Review client request to identify sample/analysis requirements, preparation methods and equipment involved

1.2

Inspect samples, compare with specifications, record and report any discrepancies

1.3

Conduct visual and simple chemical tests to identify the type of sample and sulphide concentrations

1.4

Review client sample/analysis history and identify possible chemical interferences

1.5

Decide whether non-standard fluxing is required

1.6

Select sample weight and flux to optimise precious metal recovery and purity

2

Prepare for precious metal recovery

2.1

Identify hazards and workplace safety procedures associated with the sample, preparation methods, reagents and equipment

2.2

Examine the recommended preparation method to identify the critical steps that will affect the quality of analytical results

2.3

Plan parallel work sequences to optimise the throughput of multiple sets of samples

2.4

Assemble all required equipments, materials, reagents and check they are fit for purpose

3

Recover precious metals from ore sample

3.1

Weigh required amounts of sample and flux components to achieve an acceptable button and fluid slag

3.2

Select the type and size of pot to suit sample method and client requirements

3.3

Mix charge to ensure homogeneity and optimal collection of precious metal

3.4

Set and monitor furnace temperature/time to ensure complete fusion

3.5

Separate slag and button with minimal loss of lead collector

3.6

Maintain sequencing in order to track samples, buttons and prills throughout the recovery process

3.7

Separate lead collector from the required precious metal and check for contamination, losses and evidence of other precious metals

3.8

Minimise personal exposure to hazards and the release of collectors to the work environment

3.9

Collate laboratory documentation and the prepared sample and present for analysis

4

Troubleshoot and correct failed recovery

4.1

Monitor all stages of recovery for indicators of potential loss

4.2

Recognise undesirable recovery conditions and decide whether the process requires correction

4.3

Choose an appropriate corrective action and re-start the process

4.4

Document any adjustments made to standard methods and re-sequencing of samples

4.5

Seek advice when problems are beyond scope of responsibility or knowledge

5

Perform daily maintenance of assay equipment

5.1

Segregate and dispose of waste in accordance with workplace requirements

5.2

Grade and inspect pots using established criteria prior to storage for re-use

5.3

Inspect furnaces for cracks, unserviceable components and remove slag

5.4

Inspect and clean extractive systems

5.5

Report defective equipment and consumable requirements to appropriate personnel

This field allows for different work environments and conditions that may affect performance. Essential operating conditions that may be present (depending on the work situation, needs of the candidate, accessibility of the item, and local industry and regional contexts) are included.

Standards, codes, procedures and/or workplace requirements

Standards, codes, procedures and/or workplace requirements include the latest version of one or more of:

Australian and international standards covering the requirements for the competence of testing and calibration laboratories; laboratory safety; quality and environmental management; analysis of specific ores and determination of gold; and labelling, storage, handling and transport of hazardous materials

national work health and safety (WHS) standards and codes of practice, national environmental protection measures, and national measurement regulations and guidelines

specific codes, guidelines and procedures, such as National Association of Testing Authorities (NATA) accreditation requirements, and principles of good laboratory practice (GLP)

workplace documents, such as standard operating procedures (SOPs); quality and equipment manuals; maintenance schedules; material safety data sheets (MSDS) and safety procedures; material, production and product specifications; production and laboratory schedules; workplace recording and reporting procedures; and waste minimisation and safe disposal procedures

recovery methods and procedures for specific samples, sites and clients (labelling, preparation, storage, transport and disposal), and published preparation methods

Samples

Samples include, but are not limited to, one or more of:

solids, such as rocks, minerals, soils, sands and stream sediments

core and other drill samples, such as rotary air blast (RAB), reverse circulation (RC) and aircore

slurries, powder concentrates and metallurgical solutions

dump samples and grab samples

Fluxes

Fluxes include, but are not limited to, one or more of:

bulk fluxes containing PbO, borax, soda ash, silica, silver nitrate and flour

non-standard flux additives such as:

flour (oxidising samples)

nitre (reducing samples, sulphides)

silica (basic ores)

PbO (siliceous ores)

exotic additives, such as calcium fluoride (CaF2) (refractory ores)

nickel sulphide (NiS), nickel carbonate (NiCO3), sulphur, borax and soda ash)

Sequencing of pots in a rack

Sequencing of pots in a rack includes one or more of:

addition of silver wire

addition of coloured salts, such as copper (Cu)

position of reagent blanks, standards and check samples

Collectors

Collectors include one or more of:

lead (Pb), nickel sulphide (NiS), bismuth (Bi) and tin (Sn)

Separation of collectors

Separation of collectors include one or more of:

cupellation

digestion

parting, annealing and weighing for a gravimetric finish

Waste

Waste includes, but is not limited to, one or more of:

rejected pots and cupels

slag and furnace material

disposable personal protective equipment

Hazards

Hazards include, but are not limited to, or more of:

dust, silica, slag, glass shards and molten flux

chemicals, such as hydrofluoric acid, bromine, perchloric acid, aqua regia, cyanide, lead-based compounds, free-mercury and nickel compounds

noise and vibration

crushing, entanglement and cuts associated with moving machinery

manual handling of hot/heavy loads, such as pots, racks and trolleys

heat exhaustion/stress and fatigue

Workplace safety procedures

Workplace safety procedures include, but are not limited to, one or more of:

ensuring access to service shut-off points, fire-extinguishers/fire hoses, safety showers/eye wash stations and a first aid station

recognising and observing hazard warnings and safety signs

labelling samples, reagents and hazardous materials

using direct extraction and fume hoods

providing guards for moving machinery parts

providing noise insulation

using personal protective equipment (PPE), such as dust masks, heat resistant mittens, safety face shields with tinted visor, coats, ear muffs, safety boots, heat-reflective clothing and latex gloves for flux handling

following established manual handling procedures

regularly cleaning equipment and work areas

reporting abnormal emissions, discharges and airborne contaminants, such as noise, light, solids, liquids, water/wastewater, gasses, smoke, vapour, fumes, odour and particulates, to appropriate personnel

WHS and environmental management requirements

WHS and environmental management requirements include:

· complying with WHS and environmental management requirements at all times, which may be imposed through state/territory or federal legislation. These requirements must not be compromised at any time

applying standard precautions relating to the potentially hazardous nature of samples

Evidence of competence in this unit must satisfy all of the requirements of the elements and performance criteria, and include demonstration of:

safely performing fire assay techniques to extract a range of precious metals from their host matrices in readiness for analysis on at least three (3) occasions

interpreting and closely following standard recovery methods

selecting and modifying laboratory methods to suit particular ores and to ensure total recovery

accurately weighing samples and flux components

maintaining close attention to technical and safety requirements in a physically demanding hazardous environment

maintaining sequential control of samples through all recovery stages

optimising work flow to ensure efficiency of recovery for multiple client samples

recognising and identifying the cause of non-acceptable received and fused samples, buttons and prills

identifying indicators of poor recovery and contamination

applying knowledge of mineral chemistry and fire assay techniques to solve recovery and contamination problems

keeping accurate and complete records, including:

pour sheets (date, time, client, pour number and preparation method)

number of pots, positions of sample, blank and check in rack

adjustments made to standard preparation methods for specific samples

analytical method

assay data

minimising rework, waste and environmental impacts

safely collecting and disposing of all waste responsibly

recognising hazards, using workplace safety procedures and safety equipment to work safely at all times.

Must provide evidence that demonstrates knowledge of:

chemical and physical principles relating to:

fusion of mineral ores

cupellation

parting and digestion processes

expected physical and chemical properties of materials at each recovery stage

standard methods for the fire assay of a range of precious metal ores relevant to job role

criteria for an 'acceptable' button, including:

one piece, mass >20g and <50g

malleable

separates cleanly from slag

free of undecomposed ore, matte and speiss

causes of contamination, including:

poorly made cupels

base metals (copper (Cu), nickel (Ni), zinc (Zn) and bismuth (Bi))

arsenic (As), sulphur (S), antimony (Sb), selenium (Se), tellurium (Te) and chromium (Cr)

scoria

sprouting

indicators of potential loss and the corrective actions, including:

viscous slag (check furnace temperature, adjust flux and lower charge weight)

lead shotting (adjust flux and lower charge weight to compensate for high oxides, silicates and chromites)

sulphides (adjust fusion time and adjust sample weight and/or flux)

matte, speiss (adjust sample weight and flux)

incomplete fusion (adjust sample weight and/or flux)

unacceptable button (adjust sample weight and/or flux)

inquartation (add 3 parts silver (Ag) to prill, wrap in lead foil and re-cupel)

workplace safety procedures and operation of safety equipment

function and operation of assay/equipment used as part of job role

workplace and/or legal traceability requirements

relevant hazards, work health and safety (WHS) and environment requirements.

Judgment of competence must be based on holistic assessment of the evidence. Assessment methods must confirm consistency of performance over time, rather than a single assessment event.

This unit of competency is to be assessed in the workplace or a simulated workplace environment. A simulated workplace environment must reflect realistic operational workplace conditions that cover all aspects of workplace performance, including the environment, task skills, task management skills, contingency management skills and job role environment skills.

Foundation skills are integral to competent performance of the unit and should not be assessed separately.

Assessment processes and techniques must be appropriate to the language, literacy and numeracy requirements of the work being performed and the needs of the candidate.

Knowledge evidence may be collected concurrently with performance evidence or through an independent process, such as workbooks, written assessments or interviews (provided a record is kept in each case).

This unit of competency may be assessed with:

MSL975020 Apply routine spectrometric techniques

Holistic assessment methods include:

observation of the candidate

review of quality control performance and analytical results traceable to assay samples prepared by the candidate

review of sample records prepared by the candidate

feedback from supervisors, peers and/or clients about the candidate’s ability to safely and efficiently extract a range of precious metals from their host matrices in readiness for analysis, provide acceptable buttons and prills, and troubleshoot and correct common recovery failures

written/oral questioning about relevant mineral chemistry principles, precious metal recovery steps, typical problems and corrective actions.

Access is required to instruments, equipment, materials, workplace documentation, procedures and specifications associated with this unit, including, but not limited to:

client requests/documentation, including client profile, sample identification, sample receipt, storage and analyses, and required preparation method/and service charges

a variety of precious metal ore samples

fire assay methods, examples of assay records, equipment, materials and reagents

assay equipment, including:

mixing equipment and balances

fusion and muffle furnaces and associated spares

temperature sensors and hotplates

compressed air service, extraction systems and fuel supply lines

pots, cupels, pouring equipment, pot loader, trolleys, moulds, tongs and hammers

safety equipment and workplace safety procedures.

Assessors must satisfy the assessor competency requirements that are in place at the time of the assessment as set by the VET regulator.

The assessor must demonstrate both technical competence and currency.

Technical competence can be demonstrated through:

relevant VET or other qualification/Statement of Attainment AND/OR

relevant workplace experience.

Currency can be demonstrated through:

performing the competency being assessed as part of current employment OR

having consulted with a laboratory about performing the competency being assessed within the last twelve months.

Copy and paste from the following performance criteria to create an observation checklist for each task. When you have finished writing your assessment tool every one of these must have been addressed, preferably several times in a variety of contexts. To ensure this occurs download the assessment matrix for the unit; enter each assessment task as a column header and place check marks against each performance criteria that task addresses.

Observation Checklist

Tasks to be observed according to workplace/college/TAFE policy and procedures, relevant legislation and Codes of Practice Yes No Comments/feedback
Review client request to identify sample/analysis requirements, preparation methods and equipment involved 
Inspect samples, compare with specifications, record and report any discrepancies 
Conduct visual and simple chemical tests to identify the type of sample and sulphide concentrations 
Review client sample/analysis history and identify possible chemical interferences 
Decide whether non-standard fluxing is required 
Select sample weight and flux to optimise precious metal recovery and purity 
Identify hazards and workplace safety procedures associated with the sample, preparation methods, reagents and equipment 
Examine the recommended preparation method to identify the critical steps that will affect the quality of analytical results 
Plan parallel work sequences to optimise the throughput of multiple sets of samples 
Assemble all required equipments, materials, reagents and check they are fit for purpose 
Weigh required amounts of sample and flux components to achieve an acceptable button and fluid slag 
Select the type and size of pot to suit sample method and client requirements 
Mix charge to ensure homogeneity and optimal collection of precious metal 
Set and monitor furnace temperature/time to ensure complete fusion 
Separate slag and button with minimal loss of lead collector 
Maintain sequencing in order to track samples, buttons and prills throughout the recovery process 
Separate lead collector from the required precious metal and check for contamination, losses and evidence of other precious metals 
Minimise personal exposure to hazards and the release of collectors to the work environment 
Collate laboratory documentation and the prepared sample and present for analysis 
Monitor all stages of recovery for indicators of potential loss 
Recognise undesirable recovery conditions and decide whether the process requires correction 
Choose an appropriate corrective action and re-start the process 
Document any adjustments made to standard methods and re-sequencing of samples 
Seek advice when problems are beyond scope of responsibility or knowledge 
Segregate and dispose of waste in accordance with workplace requirements 
Grade and inspect pots using established criteria prior to storage for re-use 
Inspect furnaces for cracks, unserviceable components and remove slag 
Inspect and clean extractive systems 
Report defective equipment and consumable requirements to appropriate personnel 

Forms

Assessment Cover Sheet

MSL975010 - Perform fire assay techniques
Assessment task 1: [title]

Student name:

Student ID:

I declare that the assessment tasks submitted for this unit are my own work.

Student signature:

Result: Competent Not yet competent

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Assessor name:

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Assessment Record Sheet

MSL975010 - Perform fire assay techniques

Student name:

Student ID:

Assessment task 1: [title] Result: Competent Not yet competent

(add lines for each task)

Feedback to student:

 

 

 

 

 

 

 

 

Overall assessment result: Competent Not yet competent

Assessor name:

Signature:

Date:

Student signature:

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